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目的研究建立六味地黄丸中马钱苷的薄层色谱。方法采用硅胶G薄层板,以三氯甲烷-乙酸乙酯-甲醇-甲酸(40∶5∶10∶0.2)为展开剂。制定了马钱苷的薄层鉴别。结果色谱斑点清晰,重现性好。结论该方法可以快速的鉴别马钱苷,便于基层快速检验。
Objective To study the establishment of thin layer chromatography of loganin in Liuwei Dihuang Pills. Methods Silica Gel G thin-layer plates were used with chloroform-ethyl acetate-methanol-formic acid (40:5:10:0.2) as developing solvent. A thin layer identification of curcumin was developed. As a result, the chromatographic spots were clear and the reproducibility was good Conclusion This method can quickly identify the curcumin and facilitate rapid testing at the grass roots level.