五氯酚(PCP)及五氯酚钠(PCP-Na)作为防霉剂广泛应用于木材、纸浆和皮革。本文建立皮革中PCP及PCP-Na的GLC-ECD快速测定方法,样品的前处理采用了微量化技术。该方法应用于出口皮革制品PCP测定,获得了满意的结果。 PCP and PCP-Na are widely used as preservatives in wood, pulp and leather. In this paper, GLC-ECD rapid determination method of PCP and PCP-Na in leather was established, and the sample pre-treatment was applied to the micro-quantification technology. The method was applied to the determination of PCP for export leather products and satisfactory results were obtained.