【摘 要】
：
Molybdenum( I )-compound [Mo2(SC6H11)2(CO)8] 1, crystallizes in monoclinic, space group P21/c with a = 9.5863(9), b = 9.4469(9), c = 13.869(1) A, β = 99.697(2)
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Molybdenum( I )-compound [Mo2(SC6H11)2(CO)8] 1, crystallizes in monoclinic, space group P21/c with a = 9.5863(9), b = 9.4469(9), c = 13.869(1) A, β = 99.697(2)°, V= 1238.1(2) A3, Z = 2,DC= 1.734 g/cm3, μ = 12.23 cm-1 and F(000) = 644. The finalR = 0.0455 and wR = 0.1159 for 1590 observed reflections with I> 2σ(I). 1 possesses a rhombic bimetallic core MoS2Mo with the Mo-Mo bond length of 2.975(1) and Mo-S of 2.485(2) A.
Crystallizes in monoclinic, space group P21 / c with a = 9.5863 (9), b = 9.4469 (9), c = 13.869 (1) A , β = 99.697 (2) °, V = 1238.1 (2) A3, Z = 2, DC = 1.734 g / cm3, μ = 12.23 cm -1 and F (000) = 644. The finalR = 0.0455 and wR = 0.1159 1 possesses a rhombic bimetallic core MoS2Mo with the Mo-Mo bond length of 2.975 (1) and Mo-S of 2.485 (2) A. 1590 observed reflections with I> 2σ (I).
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