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本文提出了用ICP-AES法测定马口铁中的痕量铅。试样用NaOH-H2O2溶解镀层。测得四种样品的含铅量在0.14~0.38μg/cm2范围内。方法的回收率为96.1%~103.2%。方法的精密度(RSD)为2.6%~3.8%。本法简便迅速,测量结果的准确度、精密度满足分析要求。
This paper presents the determination of trace lead in tinplate by ICP-AES. Sample with NaOH-H2O2 dissolved coating. The four samples were found to contain lead in the range of 0.14 to 0.38 μg / cm2. The recoveries of the method ranged from 96.1% to 103.2%. The precision of the method (RSD) was 2.6% ~ 3.8%. This method is simple and rapid, the accuracy of the measurement results, precision to meet the analysis requirements.