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采用甲醇法分别对罗氏海盘车、海燕、金氏真蛇尾 3种棘皮动物的皂甙进行了提取制备 ,其产率分别为 0 .0 2 33%、0 .0 52 2 %、0 .1154% ,结果表明金氏真蛇尾的皂甙含量最高 ,并且对 3种皂甙进行理化性质实验、溶血实验、紫外光谱和红外光谱鉴定比较 ,证明提取物为海星总皂甙 ,由罗氏海盘车、海燕、金氏真蛇尾提取的皂甙溶点分别为 175~ 178℃、2 4 2~ 2 55℃、2 4 4~ 2 6 0℃。
The saponins of three kinds of echinoderms of Roche, Haiyan and Jinshen were respectively extracted and prepared by methanol method, and their yields were 0. 02 33%, 0. 522.2%, 0. 1154%, respectively. The results showed that the content of saponin was the highest in Jinshizhenqi and its physicochemical properties, hemolysis experiments, UV spectra and infrared spectra were used to identify and compare the three kinds of saponins. It was proved that the extract was the total saponin of starfish, which was produced by Roche, Haiyan and Jin. The saponin’s melting points of the aspartic acid extract were 175-178°C, 242-2550°C, and 244-260°C, respectively.