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5. Synthesis and crystal structure of the trimetallic erbium tetrahydride complex [Li（THF）4][{（ButCp）2E

Synthesis and crystal structure of the trimetallic erbium tetrahydride complex [Li（THF）4][{（ButCp）2E

来源 :中国科学通报：英文版 | 被引量 : 0次 | 上传用户：syhlgs

【摘 要】

：

Reaction of [(Bu′tCp)2Er(μ-CI)]2 with Bu′Li in 1:1 molar ratio in THF at -78℃, after work-up, afforded the trimetallic erbium tetrahydride complex [Li(THF)4

【作 者】

：

YAOYingming SONGSheping SHENQi 

【机 构】

：

KeyLaboratoryofOrganicSynthesis,ChangchunInstituteofAppliedChemistry

【出 处】

：

中国科学通报：英文版

【发表日期】

：

2004年15期

【关键词】

：

铒 β-氢消除反应 晶体结构 有机镧族元素 

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Reaction of [(Bu′tCp)2Er(μ-CI)]2 with Bu′Li in 1:1 molar ratio in THF at -78℃, after work-up, afforded the trimetallic erbium tetrahydride complex [Li(THF)4][{(Bu′Cp)2Er(μ-H)}3(μ3-H)] (1) by β-hydrogen elimination reaction. Crystal structure determination

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