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微晶纤维素与异氰酸苯酯在４－Ｎ，Ｎ－二甲基氨基吡啶催化下反应合成三苯基氨基甲酸纤维素酯，反应温度低，反应时间短；以平均粒径６μｍ、平均孔径１５ｎｍ、比表面积６７ｍ２／ｇ的堆积硅珠做担体，涂敷１５％（质量分数）三苯基氨基甲酸纤维素酯在上述担体上制备手性固定相；以此手性固定相高效液相色谱法直接分离（±）－２，２，２－三氟－１－（９－蒽基）乙醇对映异构体，确定了对映异构体的出峰顺序．
Microcrystalline cellulose and phenyl isocyanate in 4-N, N- dimethylaminopyridine catalytic synthesis of triphenylcarbamate cellulose ester, the reaction temperature is low, the reaction time is short; with an average particle size of 6μm, the average A diameter of 15nm, a specific surface area of 67m2 / g deposited silica beads as a carrier, coated with 15% (mass fraction) of triphenylcarbamate prepared in the above-described carrier chiral stationary phase; the chiral stationary phase high performance liquid phase Direct separation of (±) -2,2,2-trifluoro-1- (9-anthryl) ethanol enantiomers by chromatography gave the order of peaks of the enantiomers.