Ｃ６０（ＯＨ）ｎ在生物、医药、高分子材料等许多方面具有应用前景［１～３］，其合成对Ｃ６０衍生物的水溶液化学研究与合成新的有机化合物具有重要意义．利用各种不同的方法合成出羟基个数各不相同的Ｃ６０（ＯＨ）ｎ（ｎ＝１０～２６）已有报道［４～８］，但这些方法... C60 (OH) n has potential applications in many fields such as biology, medicine and polymer materials [1 ~ 3]. The synthesis of C60 (OH) n is of great importance for the chemical research of aqueous solution of C60 derivatives and the synthesis of new organic compounds. C60 (OH) n (n = 10 ~ 26) with different number of hydroxyl groups has been reported by various methods [4-8], but these methods have been reported [...]