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本文研究了以活性炭吸附ShCl4·5H2O作催化剂合成乙酸酯的反应。对催化剂用量、醇酸比、反应时间等因素对酯收率的影响作了考察,找出了最佳酯化条件并在此条件下合成了乙酸系列酯,收率较理想。
In this paper, the reaction of activated carbon adsorption of ShCl4 · 5H2O as a catalyst for the synthesis of acetate was studied. The effect of catalyst dosage, alkyd ratio, reaction time and other factors on the yield of ester was investigated. The optimal esterification conditions were found and the acetic acid ester was synthesized under the optimum conditions.