Investigation of retention and chiral recognition mechanism using quantitative structure-enantiosele

来源 :Chinese Journal of Chemistry | 被引量 : 0次 | 上传用户:w0wchenhui
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The enantiomers of a series of fourteen O-ethyl O-(substituted) phenyl N-isopropyl-phosphoroamidothioates have been separated by high performance liquid chromatography (HPLC) on the Pirkle-type chiral stationary phase. Seven molecular descriptors were calculated and four significant descriptors were chosen to correlate against the experimental Ink’ values in order to form the quantitative structure-enann’oselectivity retention relationships (QSERRs). Through the QSERRs, the retention and enantioselectivity mechanism were examined. The enantiomers of a series of fourteen O-ethyl O- (substituted) phenyl N-isopropyl-phosphoroamidothioates have been separated by high performance liquid chromatography (HPLC) on the Pirkle-type chiral stationary phase. Seven molecular descriptors were calculated and four significant descriptors were chosen to correlate against the experimental Ink ’values ​​in order to form the quantitative structure-enann’oselectivity retention relationships (QSERRs). Through the QSERRs, the retention and enantioselectivity mechanism were examined.
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