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Five new transitional metal complexes with 4,4’-bis(1,2,4-triazol-1-ylmethyl)- biphenyl (L1), 1,4-bis(1,2,4-triazol-1-ylmethyl)naphthalene (L2) and 1-(1H-1,2,4-triazol-1-yl)-3-phenyl-2-one (L3) were synthesized and characterized by elemental analysis, IR