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Some known and new hexaaryloxyphosphazene N3P3(O-C6H4-R)6] (R=H, CH3, OCH3, C(CH3)3, CHO, F, C6H5COOR, etc) were readily obtained with ca. 70% isolated yield in refluxing acetonitrile in the presence of anhydrous potassium phosphate. All compounds were c