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A novel compound [H2Mo5.5V10.5O40 (PO4)][Cu(en)2]4·7H2O(1) was synthesized from V2O5, MoO3,CuCl2·2H2O, en, H3PO4 and H2O in an aqueous solution via the hydrothermal method and characterized by means of single-crystal X-ray diffraction, elemental