Design, synthesis and insecticidal activities of novel anthranilic diamides containing polyfluoroalk

来源 :Chinese Chemical Letters | 被引量 : 0次 | 上传用户:lbxs
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In order to discover new molecules with good insecticidal activities, a series of anthranilic diamides containing polyfluoroalkyl pyrazole were designed and synthesized, and their structures were characterized by1 H NMR and HRMS. Bioassays demonstrated that some of the title compound exhibited excellent insecticidal activities. The larvicidal activities of compound 8a, 8c, 8g, 8k and 8l against Mythimna separata Walker were 100% at 0.8 mg/L. The insecticidal activities of compound 8a, 8c,8e, 8g, 8k and 8l against Plutella xylostella Linnaeus were 100% at 0.4 mg/L. Surprisingly compounds 8a and 8c still showed 100% larvicidal activities against Plutella xylostella Linnaeus at 0.08 mg/L comparable to the commercialized Chlorantraniliprole. The LC_(50) of compound 8a and 8c against M. separata is 0.048 and 0.043 mg/L respectively. In order to discover new molecules with good insecticidal activities, a series of anthranilic diamides containing polyfluoroalkyl pyrazole were designed and synthesized, and their structures were characterized by 1 H NMR and HRMS. Bioassays said that some of the title compound exhibited excellent insecticidal activities. The larvicidal activities of compounds 8a, 8c, 8g, 8k and 8l against Mythimna separata Walker were 100% at 0.8 mg / L. The insecticidal activities of compounds 8a, 8c, 8e, 8g, 8k and 8l against Plutella xylostella Linnaeus were 100% at 0.4 mg / L. Surprisingly Compounds 8a and 8c still showed 100% larvicidal activity against Plutella xylostella Linnaeus at 0.08 mg / L comparable to the commercially available Chlorantraniliprole. The LC_ (50) of Compounds 8a and 8c against M. separata is 0.048 and 0.043 mg / L respectively.
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