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本文以大孔树脂D101、D102经吸附洗脱,薄层扫描法测定心舒通口服液中人参皂甙Rb1含量。收集70%乙醇洗脱液,浓缩后以薄层层析法分离,效果较好。展开剂:CHCl3:MeOH:H2O60:40:10。回收率为99.09%。重现性好。
In this paper, the macroporous resin D101, D102 by adsorption elution, thin-layer scanning method to determine the Xinshu Tong oral liquid ginsenoside Rb1 content. 70% ethanol eluate was collected, concentrated and separated by thin layer chromatography. The effect was better. Developing solvent: CHCl 3 : MeOH : H 2 O 60 : 40:10. The recovery rate was 99.09%. Reproducibility is good.