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本文用化学吸附硫法制备了镍硫电极，研究了活化条件对电极的催化活性及含硫量的影响，对电极表面活性层结构作了分析。
In this paper, a nickel-sulfur electrode was prepared by chemisorption sulfur method. The influence of activation conditions on the catalytic activity and sulfur content of the electrode was studied. The structure of the electrode surface active layer was analyzed.