九五年版《中国药典》硫酸阿米卡星鉴别项下〈4〉规定“取本品与硫酸阿米卡星标准品适量——供试品溶液与标准品溶液所显主斑点的颜色与位置应相 同”。笔者通过多次实验,经展开后,Rf=0,所以该方法并未起到分离作用(图1)。我们通过实验,采用下述方法,取得较好效果。 一、试剂 硫酸阿米卡星标准品(中国药品生物制品检定所) 硫酸阿米卡星原料(聊城市人民医院制剂科提 Ninety-five edition “Chinese Pharmacopoeia” Identification of amikacin <4> provisions of this product and the amount of amikacin sulfate standard - for the test solution and standard solution showed the main spots of the color and location Should be the same. " The author through many experiments, after unfolding, Rf = 0, so this method did not play a role in separation (Figure 1). We through the experiment, using the following method, to obtain better results. First, the reagent amikacin sulfate standard (China Pharmaceutical and Biological Products) sulfuric acid amikacin raw materials (Liaocheng People’s Hospital Preparation Keti