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The formation of charge transfer complexes (CTC) between C60, with metallophtha- locyanine (MPc. M=Zn. Co) has been investigated in three mixed organic solvents,The MPc-C60CTC were characterized by using UV-Vis and fluorescence spectra. The formation equilibrium constants (K) of CTC and their stoichiometry were determined.The foundation of CTC leads to a remarkable cnhancement of the photoelectrochemical property,The CTC will provide a potentialopportunity to develop a new applicable photoelectric material.