Synthesis and properties of novel soluble poly(aryl amine ketone)s as high-performance polymers

来源 :Science in China(Series B:Chemistry) | 被引量 : 0次 | 上传用户:xjqlhh0621
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
A series of poly(aryl amine ketone)s have been obtained by the condensation polymerization of different aromatic dibromides with different primary aromatic diamines via palladium-catalyzed aryl amination reaction. The structures of polymers are characterized by means of FT-IR, 1H NMR spectroscopy, and elemental analysis. The results show an agreement with the proposed structures. DSC and TG measurements show that polymers possess high glass transition temperature (Tg>170℃) and good thermal stability with high decomposition temperatures (TD>450℃). These novel polymers also exhibit good mechanical behaviors and good solubility. A series of poly (aryl amine ketone) s have been obtained by the condensation polymerization of different aromatic dibromides with different primary diamines via palladium-catalyzed aryl amination reaction. The structures of polymers are characterized by means of FT-IR, 1H NMR spectroscopy , and elemental analysis. The results show an agreement with the proposed structures. DSC and TG measurements show that polymers possess high glass transition temperature (Tg> 170 ° C) and good thermal stability with high discontinuous temperatures (TD> 450 ° C). polymers also exhibit good mechanical behaviors and good solubility.
其他文献
目的:探讨血浆内皮素1(ET1)与新生儿窒息及窒息后脑损伤的关系。方法:用放射免疫法测定20例正常足月新生儿和53例足月窒息新生儿血浆ET1浓度,并观察其动态变化(生后24小时内、第3日和第7日)。结果:患
呼和浩特炼油厂于1992 年建成投产,后来于1995 年进行催化裂化装置反再系统改造,并增加了终止剂,干气预提升,同年建成常三线油的伴气降凝装置,为消除催化裂化装置吸收稳定系统的瓶颈制约,98
急性溃疡性口腔炎是小儿时期常见的口腔粘膜疾病。临床以口颊、舌面、齿龈及上腭等处发生溃疡为特征,并常伴有明显的全身症状。任何年龄小儿均可发病,尤以2岁~4岁的婴幼儿更为
攀西层状基性-超基性岩侵入体富含大型钒钛磁铁矿床,对其已进行过详细研究。但是岩体的形成时代一直存在争议。本文采用Sm-Nd同位素年代学方法对攀枝花、白马、红格岩体的年
采用ELISA双抗体夹心法测定62例小儿肺炎及17例正常对照组血清SIL-2R活性,结果正常对照组SIL-2R为245.88±88.75U/ml。肺炎患儿为547.58±185.44U/ml;重症肺炎为679.09±138.
副理事长个人简历1960年10月1日出生于上海,1980~1990年间,在德国达姆斯塔特科技大学学习,获得物理化学博士学位,物理化学硕士学位,物理化学学士学位。专业履历
The characteristic of electrochemical oxidation of aniline on SnO 2/Ti electrode is studied. The results indicate that SnO 2/Ti electrode doped F plays a
梁某,男,7天龄。出生后哭闹不止,被认为是其他不适,6天后发现左上肢不能活动,左肘部肿胀,次日来我科就诊。检查见全身情况尚可,左肘关节处于半伸半屈位,肿胀,畸形,活动受限,扪及尺骨鹰嘴向
直肠脱垂是指肛管或直肠甚或乙状结肠外翻脱垂于肛门外,仅直肠粘膜脱垂者为不完全性脱垂,直肠壁全层脱垂者为完全性脱垂,与成人不同,小儿大部分病例不需手术,我们采用注射疗
特发性血小板减少性紫癜(ITP)是小儿常见的出血性疾病,病死率约1%,主要致死原因为颅内出血。我院血液科自1995年12月至1996年12月采用静脉输注大剂量丙种球蛋白(HDIg)及地塞