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The title adduct (C9H11N3O6, Mr = 257.21) was synthesized and it crystallizes in orthorhombic, space group P212121 with a = 5.8835(19), b = 9.517(3), c = 20.399(6) ?, V = 1142.2(6) ?3, Z = 4, Dc = 1.496 g/cm3, F(000) = 536, μ(MoKα) = 0.128 mm-1, the final R = 0.0396 and wR = 0.0800 for 1047 observed reflections with I > 2σ(I). The compound is a 1:1 adduct of dimethylamine and 3,5-dinitrobenzoic acid which are linked by hydrogen bonds to form a two-dimensional network. The dimethylamine is protonated at the nitrogen atom with the proton from the carboxyl of 3,5- dinitrobenzoic acid.
The title adduct (C9H11N3O6, Mr = 257.21) was synthesized and it crystallizes in orthorhombic space group P212121 with a = 5.8835 (19), b = 9.517 (3), c = 20.399 (6) The final R = 0.0396 and the wR = 0.0800 for 1047 are reflections with I> 2σ (I), Z = 4, Dc = 1.496 g / cm3, F (000) = 536, The compound is a 1: 1 adduct of dimethylamine and 3,5-dinitrobenzoic acid which are linked by hydrogen bonds to form a two-dimensional network. The dimethylamine is protonated at the nitrogen atom with the proton from the carboxyl of 3, 5- dinitrobenzoic acid.