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An open-framework gallophosphate, Ga9(PO4)12[(H3TREN)(H2TREN)3] ·xH2O was hydrothermally synthesized at 453K with tris(2-aminoethyl) amine (TREN) as the organic template and characterized by single-crystal X-ray diffraction. Ga9(PO4)12[(H3TREN)(H2TRE