【摘 要】
：
The title complex bis{1-(2-methoxyethyl)indenyl}dysprosium chloride ((CH3OCH2CH2C9H6)2DyCl, Mr=544.42) crystallizes in the triclinic,space group P(No.2) with un
【机 构】
：
Institute of Organic Chemistry,Fujian Institute of Research on the Structure of Matter
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The title complex bis{1-(2-methoxyethyl)indenyl}dysprosium chloride ((CH3OCH2CH2C9H6)2DyCl, Mr=544.42) crystallizes in the triclinic,space group P(No.2) with unit cell parameters a = 10.326(1), b = 10.591(1), c = 20.256(3), α = 91.543(9), β = 97.69(1), γ = 94.754(9)°, V=2186.2(9)3, Z = 4, F(000)=1076, DC=1.65g/cm3, μ=35.87cm-1, R=0.042 and Rw＝0.051 for 6193 observed reflections with I>3σ(I). X-ray crystal structure study shows there are two crystallographically independent molecules A and B (A=(CH3OCH2CH2C9H6)2 Dy(1)-Cl, B=(CH3OCH2CH2C9H6)2Dy(2)Cl) in an asymmetric unit of the title complex. Each molecule was unsolvated monomeric molecule with a trans arrangement of both the sidearms and indenyl rings.
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