论文部分内容阅读
以季戊四醇为原料，氯化亚砜为氯化剂，通过Ｖｉｌｓｍｅｉｅｒ试剂及控制它们的摩尔投料比和加料顺序，采用碱性氧化铝柱分离，一步制备出了可直接用于阳离子开环聚合的３，３-双（氯甲基）氧杂环丁烷（ＢＣＭＯ），收率为７８.９％。
Using pentaerythritol as raw material and thionyl chloride as chlorinating agent, basic alumina column was separated by Vilsmeier reagent and the mole ratio of feeding them and the order of addition, and 3 , 3-bis (chloromethyl) oxetane (BCMO) in a yield of 78.9%.