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采用正交试验法确定了直接苷化法合成辛烷基糖苷的反应条件 .实验表明选择温度1 0 0 - 1 1 0℃ ,压力 8.0 - 9.0KPa ,醇 /糖摩尔比为 3∶1为最佳反应条件 .另外 ,还相应确定了产品脱醇和漂白的适宜条件 ,并对产品生物降解等性能作了测定
Orthogonal test was used to determine the reaction conditions for the synthesis of octyl glucoside by direct glycosylation method. The experimental results showed that the optimum conditions for the synthesis of octyl glucoside were as follows: temperature 1 0-10-180 ℃, pressure 8.0-9.0 KPa, alcohol / sugar molar ratio 3:1 Good reaction conditions.In addition, the appropriate conditions for the dealcoholization and bleaching of the product were also determined, and the performance of the product such as biodegradation was determined