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@@Introduction The Baylis-Hillman (B-H) reaction is an efficient access to form C-C bond,1 In approach to accelerate the reaction rate, many physical and chemical strategies have been employed based on the different reaction system 2,3. We carried out the B-H reaction based on microreactors 3,4 in order to accelerate the reaction rate. The final products containing reactants were determined by MEKC.5