Separation and Identification of Essential Oils in Flos Caryophylli-Wenyujin by GC/MS in Different E

来源 :The 6th International Conference on Separation and Technolog | 被引量 : 0次 | 上传用户:tdkfire
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
  To compare the chemical composition of volatile oils in herbal pair Flos caryophylli-Wenyujin extracted by different polar solvents,petroleum ether,ethyl acetate,and ethanol were used in this work.The essential oils were analyzed by gas chromatography-mass spectrometry (GC/MS) [1,2].With the help of chemometric resolution method,the two-dimensional data of the overlapping peaks obtained were resolved into a pure chromatogram and a mass spectrum of each chemical compound.Different polarities of the solvents extraction of essential oils were distinct in chemical composition and relative content.44 compounds were identified in petroleum ether extraction,and the major components were Eugenol (67.38%),Caryophyllene (3.4%) and Hentriacontane (6.07%).28 compounds were identified in alcohol extraction,mainly composed of Eugenol(67.12%),Caryophyllene (10.66%) and 3-Allyl-6-methoxy-phenol (14.66%).In ethyl acetate extraction,41 compounds were identified,mainly composed of Eugenol (70.73%),Caryophyllene (8.16%) and 3-Allyl-6-methoxyphenol (9.4%).It is further demonstrated that the volatile components of herbal pair in number are almost the addition of that of two single herbs but changed in contents.
其他文献
In the present study,high-speed counter-current chromatography was applied to the systematic separation and purification of chemical components from the ethyl acetate extraction of Radix Angelicae sin
会议
The seeds of Ziziphus jujuba Mill var.spinosa (Bunge) Hu ex.H.F.Chou (Rhamnaceae,Zizyphi Spinosi Semen,ZSS) are used as a sedative medicine in China [1].In recent research,however,we found that two fl
会议
High-speed countercurrent chromatography (HSCCC) is a continuous and efficient liquid-liquid chromatography.Because there is no solid support,the separation of substances are achieved based on the dif
会议
N-methylpyrrolidine is used as raw material for synthesis of cefepime hydrochloride.A N-methylpyrrolidine group which may be decomposed from cephalosporin-ene skeleton lies in three side chain of cefe
会议
Poly (vinyl acetate-trialIyl isocyanurate-divinylbenzene) matrix coupled with oligo-β-cyclodextrin was synthesized to separate puerarin.The porous surface morphology and porous structure were investig
会议
Room Temperature Ionic Liquids (RTILs),owing to their attributes,e.g.,negligible vapor pressure,have been expected to be the green solvents which could substitute the widely used volatile organic solv
会议
A worldwide use of reverse osmosis (RO) is increasing in seawater desalination and brackish water treatment (1-4).However,many desalination plants using membrane filtration continuously have had probl
会议
Hybrid membranes of chitosan(CS)/poly(vinyl pyrrolidone)(PVP)/1,2-bis(triethoxysilyl) ethane(BTEE) were prepared via a sol-gel method for pervaporation [1-3].The membranes were characterized by Fourie
会议
Ellagic acid is currently considered for use as a cancer chemopreventive drug.It has also been reported that EA can inhibit the mutagenicity and carcinogenicity in a wide range of mutagents [1-3].EA h
会议
Recently,Korea and Japan have been investigating low-rank coal upgrading technology using solvent extraction.The solvent extraction is the technology to separate only combustible matters from low-rank
会议