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5. 石墨烯-C18增强的中空纤维液相微萃取-高效液相色谱法测定蜂蜜样品中的氯酚

石墨烯-C18增强的中空纤维液相微萃取-高效液相色谱法测定蜂蜜样品中的氯酚

来源 :2014第三届环渤海色谱质谱学术报告会 | 被引量 : 0次 | 上传用户：cys_1688

【摘 要】

：

本文将十八烷基修饰的石墨烯(G-C18)复合材料用于中空纤维液相微萃取(HF-LPME).氯酚作为模型分析物，用来评价G-C18增强的HF-LPME方法的实用性。结果表明，2-氯酚(2-chlorophenol,2-CP)和3-氯酚(3-chlorophenol, 3-CP)在5.0-200.0ng/g浓度范围内，2,3-二氯酚(2,3-dichlorophenol,2,3-DCP)和3,4-二氯

【作 者】

：

王春 臧晓欢 马小星 王志 

【机 构】

：

河北农业大学理学院化学系,河北 保定 071001

【出 处】

：

2014第三届环渤海色谱质谱学术报告会

【发表日期】

：

2014年4期

【关键词】

：

蜂蜜样品 氯酚 中空纤维液相微萃取 高效液相色谱法 石墨烯复合材料 

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论文部分内容阅读

本文将十八烷基修饰的石墨烯(G-C18)复合材料用于中空纤维液相微萃取(HF-LPME).氯酚作为模型分析物，用来评价G-C18增强的HF-LPME方法的实用性。结果表明，2-氯酚(2-chlorophenol,2-CP)和3-氯酚(3-chlorophenol, 3-CP)在5.0-200.0ng/g浓度范围内，2,3-二氯酚(2,3-dichlorophenol,2,3-DCP)和3,4-二氯酚(3,4-dichlorophenol,3,4-DCP )在2.0-200.0ng/g浓度范围内线性良好。检出限(S/N=3)低于1.5ng/g，加标回收率为88％-108%。该方法简单、有效，己成功用于测定蜂蜜样品中氯酚残留。

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