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A nanocomposite film of La0.7Sr0.3MnO3 (LSMO)-NiO has been synthesized by pulsed laser deposition (PLD).Transmission electron microscope (TEM) image shows that this nanocomposite film is about 20 nm thick.High-resolution TEM and elemental map images show the NiO nanoparticles with the mean size of 2-3 nm homogeneously distribute across the film.