In recent times,the use of plasmas,instead of more conventional catalyst synthesis methods,for a more effective preparation of catalysts has attracted a substantial amount of interest because of the unusual chemical reactivity that can be achieved in a plasma environment.[1] Therefore,a DBD plasma reactor was optimized for an innovative,non-labor intensive synthesis process for high-quality powders with catalytic activity.The method is a one-step process which results in faster and more efficient syntheses of various catalysts.