超高效液相-串联四极杆质谱联法同时测定并比较甘草各部位8种成分含量

来源 :世界中医药学会联合会中药鉴定专业委员会成立大会暨第一届学术年会 | 被引量 : 0次 | 上传用户:imoogi8406
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  建立同时检测甘草中八种成分的超高效液相-串联四极杆质谱联法(UPLC-QQQMS).样品经粉碎用甲醇(含内标液)超声提取采用安捷伦ZORBAX RRHD C18柱梯度洗脱,以ESI为离子源,采用UPLC-QQQMS动态多反应监测模式测定.结果得出,八种成分在一定范围其呈良好线性关系,相关系数均≥0.99;方法回收率范围在97.2%~113.0%间;其日内及日间相对标准偏差(RSDs)范围分别为2.63%~4.47%及1.75%~3.72%.该方法灵敏度高、稳定性强、操作简便、快捷、准确,可用于甘草各部位及其相关食品质量控制.
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