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The recent synthesis of well defined AB diblock copolymers of polystyrene (A) and polydimethylsiloxane (B) [1-4] provides an opportunity to examine the morphological properties of this unusual copolymer system.[5] We synthesized PS-b-PDMS by sequential anionic polymerization and anneal this copolymer by multi-step process (Mn=46343,Mw=59765,pdi=1.29).