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A novel complex, C44H48O8N16S2Cd2, namely, [Cd(Him)4(H2O)2][Cd(Him)4(2,6-nds)2] (Him=imidazole, 2,6-nds=2,6-naphthalenedisulfonate)], has been synthesized and structurally characterized by single-crystal X-ray diffraction. The complex crystallizes in a typical hybrid organic-inorganic pattern, and the sulfonate coordinated directly to Cd2+. Moreover, the sheet structure was formed through O-H…O and N-H…O hydrogen bonds.