Mixed-solvent thermal synthesis and magnetic properties of flower-like microstructured nickel

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Flower-like microstructured nickel was synthesized by a facile mixed-solvent thermal process.The structure,morphology,and magnetic properties of the reaction products were investigated,respectively,by X-ray diffraction (XRD),scanning electron microscopy (SEM),and vibrating sample magnetometry (VSM).The results showed that the products consisted of a face-centered cubic (fcc) structure with lattice constant of α =3.524A.The average diameter of flower-like microstructured nickel was about 5 μm and the thickness of a single flake was about 100nm.Magnetic measurement showed that these powders exhibited ferromagnetic characteristics.
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