钨酸钙是Ｘ射线和紫外线常用的发光材料，通常都用高温固相反应法合成，我们曾研究过用微波热法合成［１］．水热法是合成无机微孔材料、快离子导体等物质的重要方法，但用来合成荧光体仍少有报道．１９９０年Ｋｕｔｙ等［２，３］首次报道用水热法合成硼铝酸盐荧光体．水... Calcium tungstate is a commonly used X-ray and ultraviolet light-emitting materials, are usually synthesized by high temperature solid-state reaction, we have studied the synthesis by microwave thermal method [1]. Hydrothermal synthesis of inorganic microporous materials, fast ion conductors and other important material methods, but the synthesis of fluorescent agents is still rarely reported. Kuty et al [2,3] first reported hydrothermal synthesis of boroaluminate phosphors in 1990. water...