Fabrication and Characterization of Nano Silver Powder Prepared by Spray Pyrolysis

来源 :武汉理工大学学报(材料科学版)(英文版) | 被引量 : 0次 | 上传用户:tanshuyao
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
Silver powder was fabricated by spray pyrolysis,using 2%-20% AgNO_3 solution,336-500 mL/h flux of AgNO_3 solution,0.28-0.32 MPa flux of carrier gas and in the 620-820℃tem-perature range.The effects of furnace set temperature,concentration of AgNO_3 aqueous solution,flux of AgNO_3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder,were investigated.The experimental results showed that with the high concentration of AgNO_3 aqueous solution,the average grain size of silver decreased with the increasing of furnace set temperature.But the gain size distribution was not homogenous,the discontinuous grain growth oc-curred.With the low concentration of AgNO_3 aqueous solution,the higher furnace set temperature made the nano sliver grains sintered together to grow.Nano silver powder about 100 nm was fabricated by spray pyrolysis,using 2wt% AgNO_3 solutions,336 mL/h flux of AgNO_3 aqueous solution,0.32 MPa flux of carrier gas at 720℃ furnace set temperature.
其他文献
The precursors with NiCO_3·2Ni(OH)_2·2H2_O,Co_2(OH)_2CO_3,or both NiCO_3·2Ni(OH)_2·2H_2O and Co_2(OH)-2CO_3 coated graphite microspheres were prepared respectively by the aqueous heterogeneous precipitation using nickel sulfate,cobalt nitrate,sodium carbo
LiMn_2O_4 thin films of different thickness were derived from solution deposition and heat treated by rapid thermal annealing.The phase identification and surface morphology were studied by X-ray diffraction and scanning electron microscopy.The electroche
Amorphous nano-sized silicon nitride powders were sintered by liquid phase sin-tering.The influences of the additives of Y_2O_3 and Al_2O_3 prepared by two different ways,the poly-acrylamide gel method and the precipitation method,were investigated.The gr
The glass forming region of Bi_2O_3-B_2O_3-BaO ternary system was investigated.A serial of glass samples with high Bi2O3 content in Bi_2O_3-B_2O_3-BaO system were prepared by using conventional melting and quenching meld,and the refractive indexes and abs
A novel way for photo-immobilization with interferon-α(IFN-α)on the surface of polyurethane(PU)material,which makes PU condom more effective function in the future,was investigated.A kind of photoactive arylazide-4-azidobenzoic acid was modified to IFN-α
The biocompatibility of silicone rubber(SR)based electrodes coating with poly (vinyl alcohol)(PVA)films after implanted in the brain of rats was investigated.Twenty-two Wistar rats were used and implanted with SR electrodes and PVA/PAA films coated electr