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采用顶空-固相微萃取GC-MS法提取分析藿香正气口服液的挥发性成分,用自动质谱去卷积鉴别系统对数据进行解析。采用质谱谱库检索结合化合物保留指数定性分析色谱峰,面积归一化法进行定量分析。从藿香正气口服液中共分离出103个组分,定性鉴定了其中的80个,占总挥发性成分的94.03%。藿香正气口服液的主要挥发性成分为倍半萜烃类(51.71%)、萜醇类(24.70%)、单萜烃类(10.59%)和醛类(2.49%)等。
The volatile components of Huoxiangzhengqi Oral Liquid were extracted by headspace-solid phase microextraction and GC-MS, and the data were analyzed by automatic mass spectrometry deconvolution identification system. Qualitative analysis of chromatographic peaks using mass spectral library binding compound retention index, area normalization method for quantitative analysis. A total of 103 components were isolated from Huoxiangzhengqi Oral Liquid and 80 of them were qualitatively identified, accounting for 94.03% of the total volatile components. The main volatile components of Huoxiangzhengqi Oral Liquid are sesquiterpene hydrocarbons (51.71%), terpene alcohols (24.70%), monoterpene hydrocarbons (10.59%) and aldehydes (2.49%).