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The compound C12H19Cl2N2O·1/2H2O was obtained as the by-product of synthesizing silylene-bridged amino-oxazoline, and its structure was determined by X-ray diffraction. The crystal is of triclinic, space group P1, with a = 12.132(5), b = 12.231(5), c = 16.435(6), α = 97.485(8), β = 106.106(7), γ = 98.538(7)o, λ = 0.7103, V = 2279.0(15) 3, Z = 6, Dc = 1.251 g/cm3, Mr = 286.19, F(000) = 906, R = 0.0846 and wR = 0.2295 for 6290 observed reflections with I > 2σ(I). It is a Cl-salt. The compound was composed of phenyl, amino ion and amido derivatives. The aforementioned components were held together into a complicated three-dimensional network through three types of hydrogen bonding interactions.
The compound C12H19Cl2N2O.1 / 2H2O was obtained as the by-product of synthesizing silylene-bridged amino-oxazoline, and its structure was determined by X-ray diffraction. The crystal is of triclinic, space group P1, with a = 12.132 , b = 12.231 (5), c = 16.435 6, α = 97.485 (8), β = 106.106 (7), γ = 98.538 (7) o, λ = 0.7103, V = 2279.0 (15) Is3, Z = 6, Dc = 1.251 g / cm3, Mr = 286.19, F (000) = 906, R = 0.0846 and wR = 0.2295 for 6290 observed reflections with I> 2σ (I) The compound was composed of phenyl, amino ion and amido derivatives. The said components were held together into a complicated three-dimensional network through three types of hydrogen bonding interactions.