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目的:对市售小活络丸中松香酸进行鉴定,并研究其定量检测方法。方法:采用TLC、HPLC-PAD、HPLC-MS等对多批市售小活络丸中松香酸进行定性定量分析。结果:经检测,19批市售品中有12批检出松香酸,其含量在0.064 4~2.375 5mg·g~(-1)。结论:市售小活络丸误用混入松香的乳香、没药等原料投产现象较多,应加大监管力度。本文所建立的检测方法,可作为小活络丸的补充检验方法。
Objective: To identify rosin acid in XiaoLuoLuo Pills which is marketed, and to study its quantitative detection method. Methods: TLC, HPLC-PAD and HPLC-MS were used to qualitatively and quantitatively analyze abietic acid in Xiaowu pills. RESULTS: Twelve batches of 19 batches of commercial products were tested for abietic acid, with contents ranging from 0.064 4 to 2.375 5 mg · g -1. Conclusion: The commercial small active pills mistakenly mixed with rosin frankincense, myrrh and other raw materials put into operation more, should increase supervision and management. The detection method established in this article can be used as a supplementary test method for Xiaohuo Lo Wan.