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本文通过实验论述了在强碱条件下合成２－硝基－２′－羟基－３′，５′－二叔丁基偶氮苯的过程。ｐＨ＞１３，Ｔ＝－２℃可得到最佳收率。
In this paper, the process of synthesis of 2-nitro-2’-hydroxy-3 ’, 5’-di-tert-butylazobenzene under strong alkaline conditions was discussed experimentally. pH> 13, T = -2 ℃ can get the best yield.