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The compound phenol,2-[4(S)-4,5-dihydro-4-phenyl-2-ozazolinyl(1,C15H13NO2) was synthesized with a simple,one step method free of water and air.It was obtained in a moderate yield from the reaction of 2-hydroxybenzonitrile with optically active amino alcohol in chloroben-zene under dry,anaerobic conditions.It belongs to the orthorhombic system,space group P212121 with a = 5.786(5),b = 10.730(5),c = 19.722(5),C15H13NO2,Mr = 239.26,V = 1224.4(12)3,Z = 4 and Dc = 1.298 mg/m3.The final R = 0.0324 for 1627 observed reflections with Ⅰ > 2σ(Ⅰ) and Rw = 0.0826 for all data.The structure of compound 1 was determined by X-ray diffraction,NMR and HRMS.
The compound phenol, 2- [4 (S) -4,5-dihydro-4-phenyl- 2 -ozazolinyl (1, C15H13NO2) was synthesized with a simple, one step method of water and air moderate yield from the reaction of 2-hydroxybenzonitrile with optically active amino alcohol in chlorobenzene under dry, anaerobic conditions. At belongs to the orthorhombic system, space group P212121 with a = 5.786 (5), b = 10.730 (5), c = 19.722 (5) , C15H13NO2, Mr = 239.26, V = 1224.4 (12) 3, Z = 4 and Dc = 1.298 mg / m3.The final R = Rw = 0.0826 for all data. The structure of compound 1 was determined by X-ray diffraction, NMR and HRMS.