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A novel compound [Co(IM2-Py)2(NO3)].(NO3) (IM2-Py =2-(2'-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl) has been prepared and structurally characterized by X-ray diffraction method. It crystallizes in orthorhombic, space group P212121 with a= 11.031(