【摘 要】
：
The crystal of the title compound (C11H11 NOS2, Mr = 237.33) has been prepared and determined by X-ray single crystal diffraction. The crystal is monoclinic, sp
【机 构】
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National Key Laboratory and Institute of Elemento-Organic Chemistry
论文部分内容阅读
The crystal of the title compound (C11H11 NOS2, Mr = 237.33) has been prepared and determined by X-ray single crystal diffraction. The crystal is monoclinic, space group P21/c with parameters: a = 5. 484 (1), b = 7. 793(2), c = 28. 295(6) A, β=90.277(4)°, V =1209. 2(5) A3, Z=4, Dc=1.034 g/cm3, μ(MoKα)=0.413 mm-1 F(000) = 496 the final R = 0. 0390 and w R = 0. 1051 for 1500 observed reflections with I ＞2σ (I). The X-ray analysis result shows that the orientation of methylsulfinyl and phenyl is the cis and confirms the E-stereochemistry of the title compound.
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