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五味子对于人体有着益气、滋肾、止咳、安神等功效,因此在目前的制药行业中被广泛的采用和使用。尤其是在五酯腔囊中受到高度的重视与应用。本文就以高效液相法为主分析了测定五酯胶囊中五味子含量,并对其甲素含量进行了检测。其主要的目的在于探讨五酯腔囊中五味子甲素含量的测量方法。方法:采用AgilentC18色谱柱为主,以甲醇-水作为主要的流动相,对其流速并且进行控制使得其能够控制在1.5m·min,并且对其波长进行严格的管理和控制,形成了综合性的测量方式和测量手段。结果:五味子甲素含量得到了明确的控制与测定,其最终结果为0243～1.945ug·ml,浓度范围有着良好的线性关系。结论:高效液相色谱法在五酯胶囊五味子甲素含量测定优势与作用,其在应用的过程中有着使用方法简单、重现性良好和能够有效的测定出五味子加速含量。
Schisandra for the human body with Qi, Zishen, cough, soothe the nerves and other effects, so in the current pharmaceutical industry has been widely adopted and used. Especially in the five ester cavity capsule by a high degree of attention and application. In this paper, mainly by HPLC method for the determination of Wuzhi capsule Schisandra content, and its content of A was detected. Its main purpose is to explore the five ester cavity capsule Schisandrin content measurement method. Methods: An Agilent C18 column was used with methanol-water as the main mobile phase, its flow rate was controlled and controlled to 1.5 m · min, and the wavelength was strictly controlled and controlled to form a comprehensive Measurement methods and measurement methods. Results: The content of Schisandrin A was well controlled and determined. The final result was 0243 ~ 1.945ug · ml, and the concentration range had a good linear relationship. Conclusion: HPLC has the advantage and effect in the determination of Schisandra chinensis. Its application method is simple and reproducible, and it can effectively determine the Schisandra content.