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介绍了米诺膦酸配体的合成方法及水热法合成Cd(Ⅱ)—米诺膦酸配合物单晶的实验方法与表征手段。该实验涵盖了有机环化反应和Arbuzov反应等多种反应类型,并运用单晶衍射和波谱学技术对化合物进行表征,反映了科研型综合开放实验在教学中的成果,学科覆盖面广,可操作性强,实验效果好,有利于培养学生的综合实践能力和创新能力。
The synthesis methods of minodronic ligands and the experimental methods and characterization methods for the synthesis of Cd (II) -minogronic acid complex single crystal by hydrothermal method are introduced. This experiment covers many types of reactions such as organic cyclization reaction and Arbuzov reaction. The single crystal diffraction and spectroscopy techniques are used to characterize the compounds, which reflect the achievements of scientific research comprehensive open experiment in teaching. The discipline covers a wide range of fields and can be operated Strong, good experimental effect, is conducive to the cultivation of students’ comprehensive practical ability and innovative ability.