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目的建立高效液相色谱(HPLC)测定猪肉中氯丙嗪含量的快速、简便分析方法。方法猪肉经提取、净化处理后,利用HPLC对提取液中氯丙嗪进行分离,定量测定。结果氯丙嗪线性范围为10～100μg/ml,相关系数为0.999 8～0.999 9,回收率为95%～104%,检出限为600μg/kg,精密度为2.23%。结论该方法简便,快捷,准确,可靠,适用于测定猪肉中氯丙嗪含量尤其适合大批量样品的测定。
Objective To establish a rapid and simple method for the determination of chlorpromazine in pork by high performance liquid chromatography (HPLC). Methods After the pork was extracted and purified, the chlorpromazine in the extract was separated and determined by HPLC. Results The linear range of chlorpromazine was 10-100μg / ml, the correlation coefficient was 0.999 8-0.9999, the recovery was 95% -104%, the detection limit was 600μg / kg and the precision was 2.23%. Conclusion The method is simple, rapid, accurate and reliable. It is suitable for the determination of chlorpromazine in pork especially suitable for the determination of large quantities of samples.