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Antimony oxychloride Sb8O11Cl2(H2O)6 products with various morphologies including sheaf-like,rhombic-plate,oval leaf-like and quasi-wafer have been successfully synthesized via a mild and facile solution route at room temperature.The morphologies and structures of the as-prepared samples were characterized by X-ray powder diffraction(XRD),scanning electron microscopy(SEM) and transmission electron microscopy(TEM).A possible formation mechanism of these structures is proposed according to the experimental results and analysis.
Antimony oxychloride Sb8O11Cl2 (H2O) 6 products with various morphologies including sheaf-like, rhombic-plate, oval leaf-like and quasi-wafer have been successfully synthesized via a mild and facile solution route at room temperature. The morphologies and structures of the as -prepared samples were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). A possible formation mechanism of these structures is proposed according to the experimental results and analysis.