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The microwave synthesis of MnC_2O_4·2H_2O nanopartides was performed through the thermal double decomposition of oxalic acid dihydrate(C_2H_2O_42H_2O) and Mn(OAc)_2-4H20 solutions using a CATA-2R microwave reactor.Structural characterization was performed using X-ray diffraction(XRD),particle size and shape were analyzed using transmission electron microscopy(TEM).The chemical in the structures was investigated using electron paramagnetic resonance(EPR) as well as optical absorption spectra and near-infrared(NIR) spectroscopies.The nanocrystals produced with this method were pure and had a distorted rhombic octahedral structure.
The microwave synthesis of MnC_2O_4 · 2H_2O nanopartides was performed through the thermal double decomposition of oxalic acid dihydrate (C_2H_2O_42H_2O) and Mn (OAc) __ 2-4H20 solutions using a CATA-2R microwave reactor. Structural characterization was performed using X-ray diffraction (XRD . The chemical in the structures was investigated using electron paramagnetic resonance (EPR) as well as optical absorption spectra and near-infrared (NIR) spectroscopies. The nanocrystals produced with this method were pure and had a distorted rhombic octahedral structure.