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目的检测琥珀安神丸中添加的地西泮。方法采用C18柱,流动相为甲醇-水(70:30),检测波长254nm。结果供试品中检出地西泮。结论本方法简便、准确,为打击此类在中成药中擅自添加地西泮成份的违法行为提供技术依据。
Objective To detect the diazepam added in Amber Shenshen pill. The method used C18 column, the mobile phase was methanol-water (70:30), detection wavelength was 254nm. Results Diazepam was detected in the test sample. Conclusion This method is simple and accurate, and provides a technical basis for combating such illegal behavior of adding diazepam in Chinese patent medicine.