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The title complex, C24H36Cl2N4NiO4, crystallizes in the monoclinic system, space group P21/c with a = 15.048(3), b = 6.578(1), c = 14.405(3) ? b = 103.03(3), V = 1389.2(5) ?, Z = 2, Mr = 574.18, F(000) = 604, Dc = 1.373 g/cm3 and m(MoKa) = 0.926 mm-1. The structure was refined to R = 0.0337 and wR = 0.0954 for 2381 observed reflections (I > 2s(I)). The coordination environment around the Ni atom is a distorted NiN2O2 square-plane composed of two nitrogen and two oxygen atoms from the neutral Schiff base ligand of N-(4-hydroxylsalicylidene)-3-dimethyl- aminopropylamine
The title complex, C24H36Cl2N4NiO4, crystallizes in the monoclinic system with space group P21 / c with a = 15.048 (3), b = 6.578 (1), c = 14.405 (3)? B = 103.03 (3), V = 1389.2 5 = Z = 2, Mr = 574.18, F (000) = 604, Dc = 1.373 g / cm3 and m (MoKa) = 0.926 mm- 1. The structure was refined to R = 0.0337 and wR = 0.0954 for 2381 observed reflections (I> 2s (I)). The coordination environment around the Ni atom is a distorted NiN2O2 square-plane composed of two nitrogen and two oxygen atoms from the neutral Schiff base ligand of N- (4-hydroxylsalicylidene) -3- dimethyl-aminopropylamine