论文部分内容阅读
The surface organic modification of Fe_3O_4 nanoparticles with silane coupling reagent KH570 was studied. The modified and unmodified nanoparticles were characterized by FT-IR, XPS and TEM. The spectra of FT-IR and XPS revealed that KH570 was coated onto the surface of Fe3O4 nanoparticles to get Fe-O-Si bond and an organic coating layer also was formed. Fe3O4 nanoparticles were spheres partly with mean size of 18.8 nm studied by TEM, which was consistent with the result 17.9 nm calculated by Scherrer’s equation. KH570 was adsorbed on surface and formed chemistry bond to be steric hindrance repulsion which prevented nanoparticles from reuniting. Then glycol-based Fe_3O_4 magnetic liquids dispersed stably was gained.
The surface of modification of Fe_3O_4 nanoparticles with silane coupling reagent KH570 was studied. The modified and unmodified nanoparticles were characterized by FT-IR, XPS and TEM. The spectra of FT-IR and XPS revealed that KH570 was coated onto the surface of Fe3O4 nanoparticles to get Fe-O-Si bond and an organic coating layer also was formed. Fe3O4 nanoparticles were spheres partly with mean size of 18.8 nm studied by TEM, which was consistent with the result 17.9 nm calculated by Scherrer’s equation. and formed chemistry bond to be steric hindrance repulsion which speaks nanoparticles from reuniting. Then glycol-based Fe 3 O 4 magnetic liquids dispersed stably was gained.